3-ortho-methoxyphenyl-o-methylcarborane

Base Information

Chemical Name:3-ortho-methoxyphenyl-o-methylcarborane
CAS No.:1159494-48-0
Molecular Formula:C₁₀H₂₀B₁₀O
Molecular Weight:264.378
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-ortho-methoxyphenyl-o-methylcarborane

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Technology Process of 3-ortho-methoxyphenyl-o-methylcarborane

There total 1 articles about 3-ortho-methoxyphenyl-o-methylcarborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1159494-38-8
3-ortho-methoxyphenyl-o-carborane

: 1159494-48-0
3-ortho-methoxyphenyl-o-methylcarborane

: 1159494-44-6
3-ortho-hydroxyphenyl-o-carborane

: 1159494-46-8
3-ortho-hydroxyphenyl-o-methylcarborane

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; methylmagnesium bromide; In tetrahydrofuran; diethyl ether; Ar, a soln. of Mg compd. (8.5 equiv.) added dropwise to a soln. of B compd.and catalysts., refluxed for 34 h; quenched (dilute HCl), extd. (ethyl acetate), washed (water), dried (MgSO4), concd., chromy. (silica gel, hexane:ethyl acetate);
DOI:10.1016/j.jorganchem.2008.11.044