Technology Process of C5H3N(C5H3NCH3)C5H3NC6H5
There total 3 articles about C5H3N(C5H3NCH3)C5H3NC6H5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; copper dichloride / diethyl ether / -80 °C
2.1: n-butyllithium; tributyltin chloride / tetrahydrofuran / -78 °C
2.2: Reflux
3.1: tetrakis(triphenylphosphine) palladium(0); Na3PO4*12H2O / 1,2-dimethoxyethane; water / Reflux
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Na3PO4*12H2O; tributyltin chloride; copper dichloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; water;
1.1: Ullmann reaction / 2.2: Stille coupling / 3.1: Suzuki-Miyaura coupling;
DOI:10.1021/om300279t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium; tributyltin chloride / tetrahydrofuran / -78 °C
1.2: Reflux
2.1: tetrakis(triphenylphosphine) palladium(0); Na3PO4*12H2O / 1,2-dimethoxyethane; water / Reflux
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Na3PO4*12H2O; tributyltin chloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
1.2: Stille coupling / 2.1: Suzuki-Miyaura coupling;
DOI:10.1021/om300279t
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); Na3PO4*12H2O;
In
1,2-dimethoxyethane; water;
Reflux;
DOI:10.1021/om300279t
