Re₆Se₈(PEt₃)5(2,5-p-acetylphenyltetrazolate)(BF₄)

Base Information

• Chemical Name: Re₆Se₈(PEt₃)5(2,5-p-acetylphenyltetrazolate)(BF₄)
• CAS No.: 1384963-06-7
• Molecular Formula: BF₄*C₃₉H₈₂N₄OP₅Re₆Se₈
• Molecular Weight: 2613.7

Synonyms:

Chemical Property of Re₆Se₈(PEt₃)5(2,5-p-acetylphenyltetrazolate)(BF₄)

Chemical Property:

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Technology Process of Re₆Se₈(PEt₃)5(2,5-p-acetylphenyltetrazolate)(BF₄)

There total 1 articles about Re₆Se₈(PEt₃)5(2,5-p-acetylphenyltetrazolate)(BF₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

sodium azide + [Re6Se8(PEt3)5(p-acetylbenzonitrile)]*[BF4]2 → Re6Se8(PEt3)5(2,5-p-acetylphenyltetrazolate)(BF4) (1384963-06-7)

Guidance literature:

In nitromethane; water; Re-complex dissolved in CH3NO2, aq. soln. of NaN3 added, stirred at roomtemp. for 15 min; filtered, filtrate stipped by rotary evaporator, dissolved in CH3NO2, filtered, dripped into Et2O; elem. anal.;

DOI:10.1021/ic300877r

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