Technology Process of C14H17N3O2
There total 4 articles about C14H17N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 10h;
DOI:10.1039/c4md00505h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / 1,4-dioxane / 0.25 h / 20 °C
1.2: 10 h / 100 °C
2.1: trifluoroacetic acid / dichloromethane / 10 h / 20 °C
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane;
DOI:10.1039/c4md00505h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydroxylamine hydrochloride / ethanol / 8 h / Reflux
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / 1,4-dioxane / 0.25 h / 20 °C
2.2: 10 h / 100 °C
3.1: trifluoroacetic acid / dichloromethane / 10 h / 20 °C
With
hydroxylamine hydrochloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; ethanol; dichloromethane;
DOI:10.1039/c4md00505h
