8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

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Chemical Name:8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione
CAS No.:1422054-90-7
Molecular Formula:C₃₃H₃₁N₇O₆
Molecular Weight:621.652
Hs Code.:

8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

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Chemical Property of 8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

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Technology Process of 8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

There total 2 articles about 8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17995-04-9
N,N-bis(trimethysilyl)adenine

: 1422054-90-7
8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / Reflux

2: phosphotungstic acid / ethanol / 15 h / Reflux

With phosphotungstic acid; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2012.11.003

Reference yield:

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 1422054-90-7
8,9-dihydro-10-(9-(2-hydroxy-3-phenoxypropyl)-9H-purin-6-yl)-5-(3-hydroxyphenyl)-8,8-dimethylpyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)trione

Guidance literature:: Multi-step reaction with 3 steps

1: silica sulfuric acid / Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / Reflux

3: phosphotungstic acid / ethanol / 15 h / Reflux

With phosphotungstic acid; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2012.11.003