C₂₃H₂₃N₃O₇

Base Information

• Chemical Name: C₂₃H₂₃N₃O₇
• CAS No.: 1353338-11-0
• Molecular Formula: C₂₃H₂₃N₃O₇
• Molecular Weight: 453.452
• Mol file: 1353338-11-0.mol

Synonyms:

Chemical Property of C₂₃H₂₃N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₃N₃O₇

There total 5 articles about C₂₃H₂₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H19NO4 → C23H23N3O7 (1353338-11-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: thionyl chloride / dichloromethane / 0.5 h / 0 - 20 °C

1.2: 20 °C

2.1: triethylamine / dichloromethane / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / Inert atmosphere

4.2: Inert atmosphere

With thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/cmdc.201100372

Reference yield:

C20H25NO6 (1353337-94-6) → C23H23N3O7 (1353338-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / Inert atmosphere

2.2: Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/cmdc.201100372

Reference yield:

tert-Butyl α-ethylideneacetoacetate (64507-86-4,64507-87-5,92015-87-7) → C23H23N3O7 (1353338-11-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: N,O-bis(trimethylsilyl)hydroxylamine; zinc trifluoromethanesulfonate / dichloromethane

2.1: thionyl chloride / dichloromethane / 0.5 h / 0 - 20 °C

2.2: 20 °C

3.1: triethylamine / dichloromethane / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / Inert atmosphere

5.2: Inert atmosphere

With thionyl chloride; N,O-bis(trimethylsilyl)hydroxylamine; zinc trifluoromethanesulfonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/cmdc.201100372

upstream raw materials:

C₂₀H₂₅NO₆

C₁₆H₁₇NO₆

4-nitrobenzylamine hydrochloride

tert-Butyl α-ethylideneacetoacetate

Downstream raw materials:

C₁₆H₁₉N₃O₅