C₂₀H₂₄O₆Si

Base Information

Chemical Name:C₂₀H₂₄O₆Si
CAS No.:1446239-52-6
Molecular Formula:C₂₀H₂₄O₆Si
Molecular Weight:388.492
Hs Code.:

C<sub>20</sub>H<sub>24</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₂₀H₂₄O₆Si

Chemical Property:

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Technology Process of C₂₀H₂₄O₆Si

There total 7 articles about C₂₀H₂₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₂O₇Si

: 1446239-52-6
C₂₀H₂₄O₆Si

Guidance literature:: With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 12h;
DOI:10.1002/chem.201300702

Reference yield:

: 1446239-50-4
C₃₃H₃₀O₇Si

: 1446239-52-6
C₂₀H₂₄O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 20 °C / 760.05 Torr

2: borane-THF / tetrahydrofuran / 12 h / 0 - 20 °C

With borane-THF; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/chem.201300702

Reference yield:

: 536-74-3
phenylacetylene

: 1446239-52-6
C₂₀H₂₄O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 3.5 h / 20 °C

2.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

3.1: [RuCl₂(p-cymene)2]; water / acetonitrile / 20 °C

4.1: {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; C₅₁H₅₇F₃NO₅PS / toluene / 36 h / 25 °C / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid; sodium phosphate dibasic dodecahydrate / 1,2-dichloro-ethane / 3 h / 20 - 50 °C

6.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 20 °C / 760.05 Torr

7.1: borane-THF / tetrahydrofuran / 12 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; borane-THF; sodium phosphate dibasic dodecahydrate; [RuCl₂(p-cymene)2]; {1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}(methyl)gold; palladium 10% on activated carbon; C₅₁H₅₇F₃NO₅PS; water; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; ethyl acetate; 1,2-dichloro-ethane; toluene; acetonitrile; 4.1: |Mukaiyama Aldol Addition / 5.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1002/chem.201300702