C₃₁H₄₁FN₄O₄

Base Information

Chemical Name:C₃₁H₄₁FN₄O₄
CAS No.:1047667-00-4
Molecular Formula:C₃₁H₄₁FN₄O₄
Molecular Weight:552.689
Hs Code.:

C<sub>31</sub>H<sub>41</sub>FN<sub>4</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₁H₄₁FN₄O₄

Chemical Property:

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Technology Process of C₃₁H₄₁FN₄O₄

There total 8 articles about C₃₁H₄₁FN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂HF₃O₂*C₃₁H₄₃FN₄O₅

: 1047667-00-4
C₃₁H₄₁FN₄O₄

Guidance literature:: With N,N-diethyl-N-isopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm2007062

Reference yield:

: 1366043-02-8
C₁₂H₁₂N₂O₄S₂

: C₁₆H₂₃NO₆

: C₂₂H₂₆FNO₆

: 811867-31-9
C₂₄H₃₃NO₆

: 1047667-00-4
C₃₁H₄₁FN₄O₄

Guidance literature:: C₂₂H₂₆FNO₆; With triethylsilane; N,N-diethyl-N-isopropylamine; C₂₃H₂₂NOPolS; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; trifluoroacetic acid; In 1-methyl-pyrrolidin-2-one; dichloromethane; at 20 ℃; Inert atmosphere; solid phase reaction;

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere; solid phase reaction;

C₁₂H₁₂N₂O₄S₂; C₁₆H₂₃NO₆; C₂₄H₃₃NO₆; Further stages;
DOI:10.1021/jm2007062

Reference yield:

: C₁₇H₁₆FN₃O₂

: 1047667-00-4
C₃₁H₄₁FN₄O₄

Guidance literature:: Multi-step reaction with 7 steps

1: triphenylphosphine / tetrahydrofuran; water / 0.5 h / 40 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

3: hydrogenchloride / ethyl acetate / 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran; dichloromethane / 20 °C / Inert atmosphere

5: palladium on activated charcoal; hydrogen / ethanol / 20 °C / 1551.49 Torr / Inert atmosphere

6: triethylsilane / dichloromethane / 20 °C / Inert atmosphere

7: N,N-diethyl-N-isopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; triethylsilane; N,N-diethyl-N-isopropylamine; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole; triphenylphosphine; HATU; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/jm2007062