Technology Process of C18H15NO3S
There total 4 articles about C18H15NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; triethylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
at 20 - 105 ℃;
for 16.25h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trichlorophosphate / 0 - 5 °C
1.2: 0 - 50 °C
2.1: palladium diacetate; tris-(o-tolyl)phosphine; triethylamine / N,N-dimethyl-formamide / 16.25 h / 20 - 105 °C
With
palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; trichlorophosphate;
In
N,N-dimethyl-formamide;
1.1: |Vilsmeier-Haack Formylation / 1.2: |Vilsmeier-Haack Formylation / 2.1: |Heck Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; tris-(o-tolyl)phosphine; triethylamine / N,N-dimethyl-formamide / 16.25 h / 20 - 105 °C
2.1: trichlorophosphate / 0 - 5 °C
2.2: 0 - 50 °C
With
palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; trichlorophosphate;
In
N,N-dimethyl-formamide;
1.1: |Heck Reaction / 2.1: |Vilsmeier-Haack Formylation / 2.2: |Vilsmeier-Haack Formylation;