1,6-dichloro-3,4-diphenylisoquinoline

Base Information

Chemical Name:1,6-dichloro-3,4-diphenylisoquinoline
CAS No.:1430215-59-0
Molecular Formula:C₂₁H₁₃Cl₂N
Molecular Weight:350.247
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-dichloro-3,4-diphenylisoquinoline

Chemical Property:

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Technology Process of 1,6-dichloro-3,4-diphenylisoquinoline

There total 4 articles about 1,6-dichloro-3,4-diphenylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430215-53-4
4-butyl-6-chloro-3-(4-methoxyphenyl)-1-(2,2,2-trifluoroethoxy)isoquinoline

: 1430215-59-0
1,6-dichloro-3,4-diphenylisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / acetic acid / 2 h / 50 °C

2: trichlorophosphate / 2 h / 100 °C / Inert atmosphere

With hydrogen bromide; trichlorophosphate; In acetic acid;
DOI:10.1039/c3cc41269e

Reference yield:

: 186768-21-8
C₈H₇Cl₂NO

: 1430215-59-0
1,6-dichloro-3,4-diphenylisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: [RhCl₂(p-cymene)]2; cesium acetate / Inert atmosphere; Sealed tube

2: hydrogen bromide / acetic acid / 2 h / 50 °C

3: trichlorophosphate / 2 h / 100 °C / Inert atmosphere

With [RhCl₂(p-cymene)]2; hydrogen bromide; cesium acetate; trichlorophosphate; In acetic acid;
DOI:10.1039/c3cc41269e

Reference yield:

: 131558-77-5
4-(hexyn-1-yl)anisole

: 1430215-59-0
1,6-dichloro-3,4-diphenylisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: [RhCl₂(p-cymene)]2; cesium acetate / Inert atmosphere; Sealed tube

2: hydrogen bromide / acetic acid / 2 h / 50 °C

3: trichlorophosphate / 2 h / 100 °C / Inert atmosphere

With [RhCl₂(p-cymene)]2; hydrogen bromide; cesium acetate; trichlorophosphate; In acetic acid;
DOI:10.1039/c3cc41269e