1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Base Information

Chemical Name:1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine
CAS No.:879999-66-3
Molecular Formula:C₁₆H₁₇NO₂S
Molecular Weight:287.382
Hs Code.:

Synonyms:

Suppliers and Price of 1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

There total 4 articles about 1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4424-80-0
2,3,4,5-tetrahydro-1H-1-benzo[b]azepin-2-one

: 879999-66-3
1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminum hydride / tetrahydrofuran / 4 h / Heating

2: 4.6 g / sodium hydroxide / H₂O / Heating

With sodium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; water;
DOI:10.1080/00397910500377495

Reference yield:

: 68253-36-1
1-tetralone oxime

: 879999-66-3
1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 78.14 percent / polyphosphoric acid / 120 - 130 °C

2: lithium aluminum hydride / tetrahydrofuran / 4 h / Heating

3: 4.6 g / sodium hydroxide / H₂O / Heating

With sodium hydroxide; lithium aluminium tetrahydride; PPA; In tetrahydrofuran; water; 1: Beckmann rearrangement;
DOI:10.1080/00397910500377495

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 879999-66-3
1-benzenesulfonyl-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:: Multi-step reaction with 4 steps

1: 92.3 percent / hydroxylamine hydrochloride; pyridine / methanol / 2 h / Heating

2: 78.14 percent / polyphosphoric acid / 120 - 130 °C

3: lithium aluminum hydride / tetrahydrofuran / 4 h / Heating

4: 4.6 g / sodium hydroxide / H₂O / Heating

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; PPA; hydroxylamine hydrochloride; In tetrahydrofuran; methanol; water; 2: Beckmann rearrangement;
DOI:10.1080/00397910500377495