Pyrrolo[3,4-c]pyrrole-1-carboxylic acid, 2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-, 5-methyl-2-(1-methylethyl)cyclohexyl ester

Base Information

Chemical Name:Pyrrolo[3,4-c]pyrrole-1-carboxylic acid, 2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-, 5-methyl-2-(1-methylethyl)cyclohexyl ester
CAS No.:139255-88-2
Molecular Formula:C₃₀H₄₆N₂O₅Si
Molecular Weight:542.791
Hs Code.:

Pyrrolo[3,4-c]pyrrole-1-carboxylic acid,
2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-,
5-methyl-2-(1-methylethyl)cyclohexyl ester

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Chemical Property of Pyrrolo[3,4-c]pyrrole-1-carboxylic acid, 2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-, 5-methyl-2-(1-methylethyl)cyclohexyl ester

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Technology Process of Pyrrolo[3,4-c]pyrrole-1-carboxylic acid, 2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-, 5-methyl-2-(1-methylethyl)cyclohexyl ester

There total 4 articles about Pyrrolo[3,4-c]pyrrole-1-carboxylic acid, 2-[1,1-dimethyl-2-[(trimethylsilyl)oxy]ethyl]octahydro-4,6-dioxo-5-phenyl-, 5-methyl-2-(1-methylethyl)cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 941-69-5
N-phenyl-maleimide

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 139255-84-8
(4,4-Dimethyl-oxazolidin-3-yl)-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

: 139255-88-2
2-(1,1-Dimethyl-2-trimethylsilanyloxy-ethyl)-4,6-dioxo-5-phenyl-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: In dichloromethane; at -78 ℃; for 4h;
DOI:10.1016/S0957-4166(00)80019-1

Reference yield:

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 139255-88-2
2-(1,1-Dimethyl-2-trimethylsilanyloxy-ethyl)-4,6-dioxo-5-phenyl-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridine / tetrahydrofuran / 1 h / Ambient temperature

2: iPr₂NEt / tetrahydrofuran / 15 h / Ambient temperature

3: tetrahydrofuran / 1 h

4: 52 percent / CH₂Cl₂ / 4 h / -78 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(00)80019-1

Reference yield:

: 32815-12-6
(1S,2R,5S)-5-methyl-2-(1-methylethyl)cyclohexyl bromoacetate

: 139255-88-2
2-(1,1-Dimethyl-2-trimethylsilanyloxy-ethyl)-4,6-dioxo-5-phenyl-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: iPr₂NEt / tetrahydrofuran / 15 h / Ambient temperature

2: tetrahydrofuran / 1 h

3: 52 percent / CH₂Cl₂ / 4 h / -78 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(00)80019-1