2-amino-6-methylnicotinic acid N-oxide

Base Information

Chemical Name:2-amino-6-methylnicotinic acid N-oxide
CAS No.:1391062-88-6
Molecular Formula:C₇H₈N₂O₃
Molecular Weight:168.152
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-6-methylnicotinic acid N-oxide

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Technology Process of 2-amino-6-methylnicotinic acid N-oxide

There total 4 articles about 2-amino-6-methylnicotinic acid N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1391062-94-4
2-amino-6-methylnicotinonitrile N-oxide

: 1391062-88-6
2-amino-6-methylnicotinic acid N-oxide

Guidance literature:: 2-amino-6-methylnicotinonitrile N-oxide; With potassium hydroxide; In water; for 3h; Reflux;

With hydrogenchloride; In water; at 0 ℃; pH=4 - 5;
DOI:10.1021/jm401249c

Reference yield:

: 2-amino-6-methylnicotinonitrile N-oxide

: 1391062-88-6
2-amino-6-methylnicotinic acid N-oxide

Guidance literature:: With hydrogenchloride; In water; Microwave irradiation;

Reference yield:

: 28900-10-9
2-chloro-6-methylnicotinonitrile

: 1391062-88-6
2-amino-6-methylnicotinic acid N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / ethanol / 60 h / 180 °C / Autoclave

2: methyltrioxorhenium(VII); dihydrogen peroxide / ethanol; water / 20 h / 20 °C

3: water; hydrogenchloride / 45 h / 85 °C / 12411.9 Torr / Microwave irradiation

With hydrogenchloride; ammonia; water; dihydrogen peroxide; methyltrioxorhenium(VII); In ethanol; water;