o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

Base Information

Chemical Name:o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside
CAS No.:93677-31-7
Molecular Formula:C₅₉H₆₁NO₂₆S₂
Molecular Weight:1264.26
Hs Code.:

o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

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Chemical Property of o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

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Technology Process of o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

There total 1 articles about o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 108-24-7
acetic anhydride

: C₄₅H₄₇NO₁₉S₂

: 93677-31-7
o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1039/P19840001885

Reference yield:

: 93677-31-7
o-nitrophenyl S-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->4)-S-(2,3,6-tri-O-acetyl-4-thio-α-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-4-thio-α-D-glucopyranoside

: 93677-33-9
o-nitrophenyl 4,4'-dithio-α-maltotrioside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium methoxide, 2.) pyridine / 1.) methanol, 78 h

2: 1.) sodium methoxide, 2.) Amberlite IR 120 (H+) / 1.) methanol

With pyridine; Amberlite IR 120 (H+); sodium methylate;
DOI:10.1039/P19840001885