2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Base Information

Chemical Name:2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole
CAS No.:1599442-42-8
Molecular Formula:C₃₂H₃₉NO₃S
Molecular Weight:517.733
Hs Code.:

Synonyms:

Suppliers and Price of 2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

There total 5 articles about 2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 608-27-5
2,3-dichloroaniline

: 1599442-42-8
2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

2.1: dichloro bis(acetonitrile) palladium(II); Cy-DHTP*HBF₄; lithium tert-butoxide / toluene / 0.67 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere; Reflux

With pyridine; dichloro bis(acetonitrile) palladium(II); Cy-DHTP*HBF₄; lithium tert-butoxide; In dichloromethane; toluene;
DOI:10.1021/ol500711z

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1599442-42-8
2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

2.1: dichloro bis(acetonitrile) palladium(II); Cy-DHTP*HBF₄; lithium tert-butoxide / toluene / 0.67 h / 20 °C / Inert atmosphere

2.2: 3 h / Inert atmosphere; Reflux

With pyridine; dichloro bis(acetonitrile) palladium(II); Cy-DHTP*HBF₄; lithium tert-butoxide; In dichloromethane; toluene;
DOI:10.1021/ol500711z

Reference yield:

: 765-03-7
1-dodecyne

: 1599442-42-8
2-decyl-4-(4-methoxyphenyl)-1-tosyl-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: C₃₀H₃₅O₂P; dichloro bis(acetonitrile) palladium(II); lithium tert-butoxide / toluene / 0.67 h / 20 °C / Inert atmosphere

1.2: 3 h / Inert atmosphere; Reflux

2.1: water / toluene / 3 h / Inert atmosphere; Reflux

3.1: potassium phosphate; tetrabutyl-ammonium chloride / toluene / 12 h / Inert atmosphere; Reflux

With dichloro bis(acetonitrile) palladium(II); potassium phosphate; C₃₀H₃₅O₂P; tetrabutyl-ammonium chloride; water; lithium tert-butoxide; In toluene; 1.1: |Sonogashira Cross-Coupling / 1.2: |Sonogashira Cross-Coupling / 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.joc.6b00824