tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

Base Information

Chemical Name:tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate
CAS No.:1435944-17-4
Molecular Formula:C₁₈H₂₇NO₃
Molecular Weight:305.417
Hs Code.:

Synonyms:

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Chemical Property of tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

Chemical Property:

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Technology Process of tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

There total 5 articles about tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₅NO₃

: 1435944-17-4
tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

Guidance literature:: With diphenyl sulfide; palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃;
DOI:10.1039/c3cc40797g

Reference yield:

: 34619-03-9
tert-butyldicarbonate

: 1435944-17-4
tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 24 h / 40 °C

2: pyridinium chlorochromate; silica gel / 6 h / 20 °C

3: acetonitrile / 60 °C

4: hydrogen; palladium 10% on activated carbon; diphenyl sulfide / methanol / 20 °C

With diphenyl sulfide; palladium 10% on activated carbon; hydrogen; silica gel; pyridinium chlorochromate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1039/c3cc40797g

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 1435944-17-4
tert-butyl 2-(4,4-dimethyl-3-oxopentyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 24 h / 40 °C

2: pyridinium chlorochromate; silica gel / 6 h / 20 °C

3: acetonitrile / 60 °C

4: hydrogen; palladium 10% on activated carbon; diphenyl sulfide / methanol / 20 °C

With diphenyl sulfide; palladium 10% on activated carbon; hydrogen; silica gel; pyridinium chlorochromate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1039/c3cc40797g