C₁₂H₁₇N

Base Information

• Chemical Name: C₁₂H₁₇N
• CAS No.: 1431884-79-5
• Molecular Formula: C₁₂H₁₇N
• Molecular Weight: 175.274
• Mol file: 1431884-79-5.mol

Synonyms:

Chemical Property of C₁₂H₁₇N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₁₇N

There total 1 articles about C₁₂H₁₇N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C12H17N (1335229-15-6) → C12H17N (1431884-79-5)

Guidance literature:

With toluene-4-sulfonic acid; In water; acetonitrile; for 6h; Reflux;

DOI:10.1039/c2cc37123e

Reference yield:

C12H17N (1431884-79-5) → C17H21NO2 (1431884-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 2 h / 25 °C / Reflux

2: 1,1'-carbonyldiimidazole / chloroform / 14 h / Inert atmosphere; Reflux

With 1,1'-carbonyldiimidazole; In chloroform; toluene;

DOI:10.1039/c2cc37123e

Reference yield:

C12H17N (1431884-79-5) → C17H21NO

Guidance literature:

Multi-step reaction with 3 steps

1.1: toluene / 2 h / 25 °C / Reflux

2.1: 1,1'-carbonyldiimidazole / chloroform / 14 h / Inert atmosphere; Reflux

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 2 h / 0 °C / Inert atmosphere

With diisobutylaluminium hydride; 1,1'-carbonyldiimidazole; In hexane; dichloromethane; chloroform; toluene;

DOI:10.1039/c2cc37123e

upstream raw materials:

C₁₂H₁₇N

Downstream raw materials:

C₁₇H₂₁NO₂