6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE

Base Information

• Chemical Name: 6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE
• CAS No.: 209268-82-6
• Molecular Formula: C₁₉H₁₄N₂
• Molecular Weight: 270.334
• Mol file: 209268-82-6.mol

Synonyms:

Chemical Property of 6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE

Chemical Property:

Purity/Quality:

6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE

There total 4 articles about 6,13-DIHYDRO-5H-INDOLO[3,2-C]ACRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,3-dihydro-1H-acridin-4-one-phenylhydrazone (49568-12-9) → 12,13-dihydro-5H-indolo[3,2-c]acridine (209268-82-6)

Guidance literature:

With PPA; at 120 ℃; for 0.5h;

DOI:10.1021/jo980134j

Reference yield:

4-oxo-1,2,3,4-tetrahydroacridine (49568-10-7) → 12,13-dihydro-5H-indolo[3,2-c]acridine (209268-82-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / AcOH / ethanol / 2 h / Heating

2: 70 percent / PPA / 0.5 h / 120 °C

With acetic acid; In ethanol;

DOI:10.1021/jo980134j

Reference yield:

1,2,3,4-tetrahydroacridine (3295-64-5) → 12,13-dihydro-5H-indolo[3,2-c]acridine (209268-82-6)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium ethylate; diethyl ether; ethanol

2: pyridine / und anschliessend mit einer aus Anilin hergestellten wss.Diazoniumsalz-Loesung

3: ethanolic HCl

With pyridine; hydrogenchloride; diethyl ether; ethanol; potassium ethoxide;

upstream raw materials:

2,3-dihydro-1H-acridin-4-one-phenylhydrazone

4-oxo-1,2,3,4-tetrahydroacridine

1,2,3,4-tetrahydroacridine