2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

Base Information

Chemical Name:2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide
CAS No.:54610-37-6
Molecular Formula:C₁₈H₂₂N₂O
Molecular Weight:282.385
Hs Code.:

2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopenta<c>pyrrole-4-carboxamide

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Chemical Property of 2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

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Technology Process of 2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

There total 9 articles about 2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54609-27-7
1,3,4,6,6-pentamethyl-2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]pyrrole-4-carbonitrile

: 54610-37-6
2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / SO₂Cl₂ / CCl₄ / Ambient temperature

2: 25 percent / TFA / 3 h / Heating

3: 91percent H₂SO₄ / Ambient temperature

4: 0.1 g / 10percent Pd/C / various solvent(s) / 2 h / Heating

With palladium on activated charcoal; sulfuryl dichloride; sulfuric acid; trifluoroacetic acid; In tetrachloromethane;
DOI:10.1021/jm00182a024

Reference yield:

: 54610-35-4
2-phenyl-3-formyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopenta[c]-pyrrole-4-carboxamide

: 54610-37-6
2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

Guidance literature:: With palladium on activated charcoal; In various solvent(s); for 2h; Heating;
DOI:10.1021/jm00182a024

Reference yield:

: 54609-78-8
1-formyl-2-phenyl-2,4,5,6-tetrahydro-4,6,6-tetramethylcyclopentapyrrole-4-carbonitrile

: 54610-37-6
2-phenyl-2,4,5,6-tetrahydro-1,4,6,6-tetramethylcyclopentapyrrole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / KOH, N₂H_4.H₂O / various solvent(s)

2: 1.) N,N'-carbonyldiimidiazole, 2.) NH₃ / 1.) THF, RT, 6 h, 2.) THF, 18 h

With potassium hydroxide; ammonia; hydrazine hydrate; 1,1'-carbonyldiimidazole; In various solvent(s);
DOI:10.1021/jm00182a024