C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾
CAS No.:1427578-73-1
Molecular Formula:C₁₄H₉N₂O₅S*Na
Molecular Weight:340.292
Hs Code.:

C<sub>14</sub>H<sub>9</sub>N<sub>2</sub>O<sub>5</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:

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Chemical Property of C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

There total 3 articles about C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911417-23-7
2-(3-hydroxylphenyl)quinazolin-4(3H)-one

: 1427578-73-1
C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: 2-(3-hydroxylphenyl)quinazolin-4(3H)-one; With sulfur trioxide trimethylamine complex; triethylamine; In acetonitrile; at 90 ℃; for 0.5h; Microwave irradiation;

DOI:10.1021/jm301757v

Reference yield:

: 28144-70-9,88-68-6
anthranilic acid amide

: 1427578-73-1
C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogen sulfate / N,N-dimethyl acetamide / 12 h / 145 °C

2.1: sulfur trioxide trimethylamine complex; triethylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

2.2: SP Sephadex C-25 column

With sodium hydrogen sulfate; sulfur trioxide trimethylamine complex; triethylamine; In N,N-dimethyl acetamide; acetonitrile;
DOI:10.1021/jm301757v

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 1427578-73-1
C₁₄H₉N₂O₅S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogen sulfate / N,N-dimethyl acetamide / 12 h / 145 °C

2.1: sulfur trioxide trimethylamine complex; triethylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

2.2: SP Sephadex C-25 column

With sodium hydrogen sulfate; sulfur trioxide trimethylamine complex; triethylamine; In N,N-dimethyl acetamide; acetonitrile;
DOI:10.1021/jm301757v