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Technology Process of Hg(Se-2-t-BuCONHC6H4)2

Hg(Se-2-t-BuCONHC6H4)2

Base Information
  • Chemical Name:Hg(Se-2-t-BuCONHC6H4)2
  • CAS No.:915945-20-9
  • Molecular Formula:C22H28HgN2O2Se2
  • Molecular Weight:710.987
  • Hs Code.:
Hg(Se-2-t-BuCONHC<sub>6</sub>H<sub>4</sub>)2

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Chemical Property of Hg(Se-2-t-BuCONHC6H4)2
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Technology Process of Hg(Se-2-t-BuCONHC6H4)2

There total 1 articles about Hg(Se-2-t-BuCONHC6H4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

bis(2-pivaloylaminophenyl)diselenide
915945-21-0

bis(2-pivaloylaminophenyl)diselenide

mercury dichloride

mercury dichloride

Hg(Se-2-t-BuCONHC<sub>6</sub>H<sub>4</sub>)2
915945-20-9

Hg(Se-2-t-BuCONHC6H4)2

Guidance literature:
With sodium borohydride; In methanol; under Ar atm. to soln. diselenide in MeOH NaBH4 was added and stirred for 5 min, acetic acid was added, HgCl2 was added and stirred for 3 h; soln. was concd. in vacuo, aq. NaCl was added, org. layer was separated and washed with aq. HCl, aq. NaHCO3, water and aq. NaCl and dried over Na2SO4, soln. was concd. in vacuo and recrystd. from Et2O - n-hexane; elem. anal.;
DOI:10.1021/ic061140y
upstream raw materials:

bis(2-pivaloylaminophenyl)diselenide

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