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Technology Process of C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3

C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3

Base Information
  • Chemical Name:C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3
  • CAS No.:1393659-97-6
  • Molecular Formula:C45H71N3PTa
  • Molecular Weight:866
  • Hs Code.:
C<sub>6</sub>H<sub>11</sub>PTa(N(CH<sub>2</sub>C(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)3

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Technology Process of C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3

There total 2 articles about C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

ClTa(N(CH<sub>2</sub>C(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)2(N(C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)CH(C(CH<sub>3</sub>)3))

ClTa(N(CH2C(CH3)3)C6H3(CH3)2)2(N(C6H3(CH3)2)CH(C(CH3)3))

lithium cyclohexylphosphanide

lithium cyclohexylphosphanide

C<sub>6</sub>H<sub>11</sub>PTa(N(CH<sub>2</sub>C(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)3
1393659-97-6

C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3

Guidance literature:
In benzene; Ta compd. treated with Li compd. in C6H6 for 18 h;
DOI:10.1039/c2dt31082a

Reference yield:

TaH(η2-N(3,5-dimethylphenyl)CHtBu)(N(3,5-dimethylphenyl)CH2tBu)2

TaH(η2-N(3,5-dimethylphenyl)CHtBu)(N(3,5-dimethylphenyl)CH2tBu)2

C<sub>6</sub>H<sub>11</sub>PTa(N(CH<sub>2</sub>C(CH<sub>3</sub>)3)C<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)3
1393659-97-6

C6H11PTa(N(CH2C(CH3)3)C6H3(CH3)2)3

Guidance literature:
Multi-step reaction with 2 steps
1: chloroform
2: benzene
In chloroform; benzene;
DOI:10.1039/c2dt31082a
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