Technology Process of C16H11ClN4O3S
There total 8 articles about C16H11ClN4O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 99 percent / NH2OH*HCl; aq. NaOAc / ethanol
2: 92 percent / pyridine
3: 60 percent / aq. KOAc / ethanol
4: 91 percent / BH3*S(CH3)2 / tetrahydrofuran
5: Et3N / CH2Cl2
6: aq. KMnO4; MgSO4 / acetone / 70 °C
8: NH2NH2
With
pyridine; potassium permanganate; dimethylsulfide borane complex; hydroxylamine hydrochloride; potassium acetate; sodium acetate; magnesium sulfate; triethylamine; hydrazine;
In
tetrahydrofuran; ethanol; dichloromethane; acetone;
1: Condensation / 2: Tosylation / 3: Rearrangement / 4: Reduction / 5: Acylation / 6: Oxidation / 7: Alkylation / 8: Cyclization;
DOI:10.1016/S0960-894X(00)00084-6
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 92 percent / pyridine
2: 60 percent / aq. KOAc / ethanol
3: 91 percent / BH3*S(CH3)2 / tetrahydrofuran
4: Et3N / CH2Cl2
5: aq. KMnO4; MgSO4 / acetone / 70 °C
7: NH2NH2
With
pyridine; potassium permanganate; dimethylsulfide borane complex; potassium acetate; magnesium sulfate; triethylamine; hydrazine;
In
tetrahydrofuran; ethanol; dichloromethane; acetone;
1: Tosylation / 2: Rearrangement / 3: Reduction / 4: Acylation / 5: Oxidation / 6: Alkylation / 7: Cyclization;
DOI:10.1016/S0960-894X(00)00084-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / BH3*S(CH3)2 / tetrahydrofuran
2: Et3N / CH2Cl2
3: aq. KMnO4; MgSO4 / acetone / 70 °C
5: NH2NH2
With
potassium permanganate; dimethylsulfide borane complex; magnesium sulfate; triethylamine; hydrazine;
In
tetrahydrofuran; dichloromethane; acetone;
1: Reduction / 2: Acylation / 3: Oxidation / 4: Alkylation / 5: Cyclization;
DOI:10.1016/S0960-894X(00)00084-6