C₃₂H₅₀N₂

Base Information

Chemical Name:C₃₂H₅₀N₂
CAS No.:1285370-69-5
Molecular Formula:C₃₂H₅₀N₂
Molecular Weight:462.762
Hs Code.:

C<sub>32</sub>H<sub>50</sub>N<sub>2</sub>

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Chemical Property of C₃₂H₅₀N₂

Chemical Property:

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Technology Process of C₃₂H₅₀N₂

There total 7 articles about C₃₂H₅₀N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285370-68-4
C₃₂H₄₈N₂

: 1285370-69-5
C₃₂H₅₀N₂

Guidance literature:: C₃₂H₄₈N₂; With n-butyllithium; In tetrahydrofuran; hexane; at -30 ℃; for 1h;

With iodine; In 2-methyltetrahydrofuran; at -115 ℃; for 1h;
DOI:10.1021/ja200708b

Reference yield:

: 1285370-63-9
C₂₂H₃₂N₂

: 1285370-69-5
C₃₂H₅₀N₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on carbon; hydrogen / acetic acid / 24 h

2.1: N-Bromosuccinimide; sodium sulfate; sodium hydrogencarbonate / chloroform / 3 h / -40 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; benzene / 24 h / 90 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 °C

4.2: 1 h / -115 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium on carbon; sodium sulfate; hydrogen; sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; ethanol; hexane; chloroform; water; acetic acid; benzene; 3.1: Suzuki coupling;
DOI:10.1021/ja200708b

Reference yield:

: 1285370-65-1
C₂₂H₃₆N₂

: 1285370-69-5
C₃₂H₅₀N₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; sodium sulfate; sodium hydrogencarbonate / chloroform / 3 h / -40 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; benzene / 24 h / 90 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 °C

3.2: 1 h / -115 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium sulfate; sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; ethanol; hexane; chloroform; water; benzene; 2.1: Suzuki coupling;
DOI:10.1021/ja200708b