C₃₀H₂₄BrClNO₂P

Base Information

• Chemical Name: C₃₀H₂₄BrClNO₂P
• CAS No.: 1516972-60-3
• Molecular Formula: C₃₀H₂₄BrClNO₂P
• Molecular Weight: 576.857
• Mol file: 1516972-60-3.mol

Synonyms:

Chemical Property of C₃₀H₂₄BrClNO₂P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₄BrClNO₂P

There total 4 articles about C₃₀H₂₄BrClNO₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,6-chrysenedione (2051-10-7) → C30H24BrClNO2P (1516972-60-3)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphorus trichloride

2: bromine / chloroform / 8 h / 20 - 25 °C / Inert atmosphere

3: chloroform / 2 h / Inert atmosphere; Reflux

With bromine; phosphorus trichloride; In chloroform;

DOI:10.1134/S1070428013110109

Reference yield:

phenylacetylene (536-74-3) → C30H24BrClNO2P (1516972-60-3)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphorus trichloride

2: bromine / chloroform / 8 h / 20 - 25 °C / Inert atmosphere

3: chloroform / 2 h / Inert atmosphere; Reflux

With bromine; phosphorus trichloride; In chloroform;

DOI:10.1134/S1070428013110109

Reference yield:

4-phenyl-2,7-dichloro-2-chryseno[6,5-e][1,2]phosphinine 2-oxide (881171-56-8) → C30H24BrClNO2P (1516972-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / chloroform / 8 h / 20 - 25 °C / Inert atmosphere

2: chloroform / 2 h / Inert atmosphere; Reflux

With bromine; In chloroform;

DOI:10.1134/S1070428013110109

upstream raw materials:

5,6-chrysenedione

phenylacetylene

4-phenyl-2,7-dichloro-2-chryseno[6,5-e][1,2]phosphinine 2-oxide

C₂₆H₁₄BrCl₂O₂P

Downstream raw materials:

C₂₆H₁₅BrClO₃P*C₄H₁₁N