DPZOH

Base Information

• Chemical Name: DPZOH
• CAS No.: 1080632-98-9
• Molecular Formula: C₁₃H₁₂N₂O
• Molecular Weight: 223.164
• Mol file: 1080632-98-9.mol

Synonyms:

Chemical Property of DPZOH

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of DPZOH

There total 1 articles about DPZOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

nitrosobenzene-d5 (18628-43-8) + 4-H2N-C6D4-CD2-OH (1080632-97-8) → DPZOH (1080632-98-9)

Guidance literature:

With acetic acid; at 0 - 20 ℃; for 2h;

DOI:10.1039/b804568b

Reference yield: 63.0%

bis(trichloromethyl) carbonate (32315-10-9) + DPZOH (1080632-98-9) → [D11]-4-phenylazo benzyl chloroformate (1080632-99-0)

Guidance literature:

In 1,4-dioxane; at 15 - 40 ℃;

DOI:10.1039/b804568b

upstream raw materials:

nitrosobenzene-d₅

4-H₂N-C₆D₄-CD₂-OH

Downstream raw materials:

[D₁₁]-4-phenylazo benzyl chloroformate