Technology Process of C70H90N4O6
There total 5 articles about C70H90N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
terephthaloyl chloride;
With
pyridine;
for 0.0333333h;
Inert atmosphere;
C31H44N4O2;
at 115 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja500607d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
2.1: pyridine / 0.03 h / Inert atmosphere
2.2: 12 h / 115 °C / Inert atmosphere
With
pyridine; sodium azide; ammonium chloride;
In
N,N-dimethyl-formamide;
DOI:10.1021/ja500607d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h
1.2: 12 h / 100 °C
2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
2.2: 3 h / 25 °C / Inert atmosphere
3.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
4.1: pyridine / 0.03 h / Inert atmosphere
4.2: 12 h / 115 °C / Inert atmosphere
With
pyridine; sodium azide; sodium hydride; potassium carbonate; ammonium chloride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja500607d