β-(S-benzylmercapto)-β,β-diethylpropionic acid

Base Information

• Chemical Name: β-(S-benzylmercapto)-β,β-diethylpropionic acid
• CAS No.: 36038-80-9
• Molecular Formula: C₁₄H₂₀O₂S
• Molecular Weight: 252.378

Synonyms:

Chemical Property of β-(S-benzylmercapto)-β,β-diethylpropionic acid

Chemical Property:

Purity/Quality:

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Technology Process of β-(S-benzylmercapto)-β,β-diethylpropionic acid

There total 2 articles about β-(S-benzylmercapto)-β,β-diethylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentan-3-one (96-22-0) → β-(S-benzylmercapto)-β,β-diethylpropionic acid (36038-80-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn / benzene; toluene

2: (i) P₂O₅, benzene, (ii) /BRN= 605864/, piperidine

With zinc; In toluene; benzene;

DOI:10.1021/jm00272a001

Reference yield:

Ethyl 3-ethyl-3-hydroxypentanoate (22624-32-4) + phenylmethanethiol (100-53-8) → β-(S-benzylmercapto)-β,β-diethylpropionic acid (36038-80-9)

Guidance literature:

Multistep reaction; (i) P₂O₅, benzene, (ii) /BRN= 605864/, piperidine;

DOI:10.1021/jm00272a001

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + β-(S-benzylmercapto)-β,β-diethylpropionic acid (36038-80-9) → β-(S-Benzylmercapto)-β,β-diaethylpropionsaeure-p-nitrophenylester (52192-19-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In ethyl acetate;

DOI:10.1021/jm00248a028

upstream raw materials:

Ethyl 3-ethyl-3-hydroxypentanoate

phenylmethanethiol

pentan-3-one

Downstream raw materials:

β-(S-Benzylmercapto)-β,β-diaethylpropionsaeure-p-nitrophenylester

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