C₂₇H₃₆O₇

Base Information

Chemical Name:C₂₇H₃₆O₇
CAS No.:1263362-14-6
Molecular Formula:C₂₇H₃₆O₇
Molecular Weight:472.579
Hs Code.:

C<sub>27</sub>H<sub>36</sub>O<sub>7</sub>

Synonyms:

Suppliers and Price of C₂₇H₃₆O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₆O₇

Chemical Property:

Purity/Quality:

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Technology Process of C₂₇H₃₆O₇

There total 12 articles about C₂₇H₃₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₄O₅

: 1263362-14-6
C₂₇H₃₆O₇

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In 1,4-dioxane; tert-butyl alcohol; at 20 ℃; for 17h;
DOI:10.1021/jo1022102

Reference yield:

: 1263362-58-8
C₁₆H₁₅BrO₄

: 1263362-14-6
C₂₇H₃₆O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: lithium borohydride / diethyl ether / 20.5 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / hexanes; diethyl ether / 15 h / Inert atmosphere; Cooling

3.2: 0.25 h / Inert atmosphere; Cooling

3.3: 20 °C / Inert atmosphere; Cooling

4.1: boron trifluoride diethyl etherate / dichloromethane / 0.13 h / -78 °C / Inert atmosphere

4.2: 23 h / 20 °C / 760.05 Torr

5.1: manganese(IV) oxide / dichloromethane / 20 h / 20 °C / Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.2: 20 h / 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 26 h / 20 °C / Inert atmosphere

9.1: potassium hydroxide / ethanol / 0.42 h / 20 °C / Inert atmosphere

10.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane / 2 h / 20 °C / Inert atmosphere

11.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane; tert-butyl alcohol / 17 h / 20 °C

With manganese(IV) oxide; sodium tetrahydroborate; osmium(VIII) oxide; lithium borohydride; n-butyllithium; tetrapropylammonium perruthennate; N,N,N,N,-tetramethylethylenediamine; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; water; sodium hydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; hexanes; diethyl ether; ethanol; dichloromethane; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo1022102

Reference yield:

: C₂₇H₃₂O₅

: 1263362-14-6
C₂₇H₃₆O₇

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane; tert-butyl alcohol / 17 h / 20 °C

With sodium tetrahydroborate; osmium(VIII) oxide; cerium(III) chloride heptahydrate; water; 4-methylmorpholine N-oxide; In 1,4-dioxane; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jo1022102