bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium

Base Information

• Chemical Name: bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium
• CAS No.: 1219023-97-8
• Molecular Formula: C₈N₄NiS₄*C₁₆H₁₂BrClN
• Molecular Weight: 672.704

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Chemical Property of bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium

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Technology Process of bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium

There total 1 articles about bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

[1-(2'-chloro-4'-bromobenzyl)-isoquinolinium]2[Ni(maleonitriledithiolate)2] → bis(maleonitriledithiolato)Ni(III) 1-(2'-chloro-4'-bromobenzyl)-isoquinolinium (1219023-97-8)

Guidance literature:

With I₂; In acetonitrile; Ni(II) complex (BrClBzIQl)2(Ni(mnt)2 solved in MeCN; soln. I2 (MeCN) added; mixt. stirred for 12 h at room temp.; CH3OH added; stand overnight;; crystals filtered off, washed (CH3OH, Et2O); dried in vac.; elem. anal.;

DOI:10.1080/15533170903129729

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