Technology Process of C14H17N3O5S
There total 5 articles about C14H17N3O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: toluene-4-sulfonic acid / acetonitrile
2: diisobutylaluminium hydride / diethyl ether / -78 °C
3: pyridine / dichloromethane / 1 h / -20 °C
4: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
5: ammonium cerium (IV) nitrate
6: dmap / 1,2-dichloro-ethane
7: toluene-4-sulfonic acid; water / acetonitrile; methanol
With
pyridine; dmap; sodium azide; ammonium cerium (IV) nitrate; water; diisobutylaluminium hydride; toluene-4-sulfonic acid;
In
methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: diisobutylaluminium hydride / diethyl ether / -78 °C
2: pyridine / dichloromethane / 1 h / -20 °C
3: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
4: ammonium cerium (IV) nitrate
5: dmap / 1,2-dichloro-ethane
6: toluene-4-sulfonic acid; water / acetonitrile; methanol
With
pyridine; dmap; sodium azide; ammonium cerium (IV) nitrate; water; diisobutylaluminium hydride; toluene-4-sulfonic acid;
In
methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap / 1,2-dichloro-ethane
2: toluene-4-sulfonic acid; water / acetonitrile; methanol
With
dmap; water; toluene-4-sulfonic acid;
In
methanol; 1,2-dichloro-ethane; acetonitrile;
