Technology Process of phenyl 2,3,5-trimethoxybenzyl sulfone
There total 5 articles about phenyl 2,3,5-trimethoxybenzyl sulfone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 82 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 6 h / Heating; Irradiation
2: 1.) BuLi / 1.) THF, hexane, 5 min, 2.) THF, hexane, 0 deg C, 2 h
3: tetrahydrofuran; hexane / 2 h / -78 °C
4: m-chloroperbenzoic acid / CH2Cl2 / 0.5 h / Heating
With
N-Bromosuccinimide; n-butyllithium; Perbenzoic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; tetrachloromethane; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) BuLi / 1.) THF, hexane, 5 min, 2.) THF, hexane, 0 deg C, 2 h
2: tetrahydrofuran; hexane / 2 h / -78 °C
3: m-chloroperbenzoic acid / CH2Cl2 / 0.5 h / Heating
With
n-butyllithium; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 76 percent / NaOH / methanol; H2O / 1 h / Ambient temperature
2: 82 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 6 h / Heating; Irradiation
3: 1.) BuLi / 1.) THF, hexane, 5 min, 2.) THF, hexane, 0 deg C, 2 h
4: tetrahydrofuran; hexane / 2 h / -78 °C
5: m-chloroperbenzoic acid / CH2Cl2 / 0.5 h / Heating
With
sodium hydroxide; N-Bromosuccinimide; n-butyllithium; Perbenzoic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; tetrachloromethane; hexane; dichloromethane; water;
