CRu₆(CO)15(P(CH₃)2C₆H₅)2

Base Information

• Chemical Name: CRu₆(CO)15(P(CH₃)2C₆H₅)2
• CAS No.: 460986-57-6
• Molecular Formula: C₃₂H₂₂O₁₅P₂Ru₆
• Molecular Weight: 1314.89

Synonyms:

Chemical Property of CRu₆(CO)15(P(CH₃)2C₆H₅)2

Chemical Property:

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Technology Process of CRu₆(CO)15(P(CH₃)2C₆H₅)2

There total 2 articles about CRu₆(CO)15(P(CH₃)2C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbido heptadecacarbonyl hexaruthenium + Dimethyl(phenyl)phosphine (672-66-2) → CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6) + CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6)

Guidance literature:

In dichloromethane; (N2); stirring a soln. of ruthenium cluster and phosphine in CH2Cl2 at room temp. for 10 min; evapn., thin layer chromy. (SiO2, hexane/CH2Cl2, 3:1); obtained as a mixt. of isomers;

DOI:10.1016/S0022-328X(02)01368-2

Reference yield:

carbido heptadecacarbonyl hexaruthenium + Dimethyl(phenyl)phosphine (672-66-2) → CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6) + CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6)

Guidance literature:

In dichloromethane; (N2); stirring a soln. of ruthenium cluster and phosphine in CH2Cl2 at room temp. for 10 min; evapn., thin layer chromy. (SiO2, hexane/CH2Cl2, 3:1); obtained as a mixt. of isomers;

DOI:10.1016/S0022-328X(02)01368-2

Reference yield: 11.0%

CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6) + CRu6(CO)15(P(CH3)2C6H5)2 (460986-51-0,460986-57-6) → CRu6(CO)13(P(CH3)2)((CH3)2PC6H4) + CRu6(CO)14(P(CH3)2C6H5)(CH3C6H5PCH2)H

Guidance literature:

With (CH₃)3NO*2H₂O; In dichloromethane; (N2);stirring a soln. of ruthenium cluster and amine oxide in CH2Cl2 at room temp. for 1 h; evapn., thin layer chromy (SiO2, hexane/CH2Cl2 3:1); elem. anal.;

DOI:10.1016/S0022-328X(02)01368-2

upstream raw materials:

Dimethyl(phenyl)phosphine

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