1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

Base Information

Chemical Name:1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine
CAS No.:141944-49-2
Molecular Formula:C₂₅H₂₄N₂
Molecular Weight:352.479
Hs Code.:

1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzo<j>phenanthridinamine

Synonyms:

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Chemical Property of 1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

Chemical Property:

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Technology Process of 1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

There total 6 articles about 1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 141944-42-5
N-<2-(dimethylamino)-6-(2-naphthalenyl)-3-cyclohexen-1-yl>benzamide

: 141944-49-2
1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

Guidance literature:: With trichlorophosphate; for 1.5h; Heating;
DOI:10.1002/jhet.5570290106

Reference yield:

: 139943-10-5,1515-77-1
N,N-dimethyl-1,3-butadien-1-amine

: 141944-49-2
1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: glacial acetic acid, Zn / 20 h / Ambient temperature

3: 50 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

4: 60 percent / POCl₃ / 1.5 h / Heating

With sodium hydroxide; acetic acid; hydroquinone; zinc; trichlorophosphate; In chloroform;
DOI:10.1002/jhet.5570290106

Reference yield:

: 37629-37-1,21461-46-1
2-(2-nitrovinyl)naphthalene

: 141944-49-2
1,4,4a,10b-tetrahydro-N,N-dimethyl-4-benzophenanthridinamine

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: glacial acetic acid, Zn / 20 h / Ambient temperature

3: 50 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

4: 60 percent / POCl₃ / 1.5 h / Heating

With sodium hydroxide; acetic acid; hydroquinone; zinc; trichlorophosphate; In chloroform;
DOI:10.1002/jhet.5570290106