(2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

Base Information

Chemical Name:(2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate
CAS No.:1433187-97-3
Molecular Formula:C₁₉H₁₉NO₃S₂
Molecular Weight:373.497
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

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Technology Process of (2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

There total 5 articles about (2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 3966-32-3
(R)-methoxyphenylacetic acid

: 244221-77-0
(R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-ol

: 1433187-97-3
(2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tet.2013.04.014

Reference yield:

: 23385-34-4
1-(benzothiazol-2-ylthio)propan-2-one

: 1433187-97-3
(2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 2 h / 0 - 5 °C / Inert atmosphere

2: amano PS (native lipase from B_. cepacia earlier Pseudomonas cepacia) / toluene / 306 h / 32 °C / Resolution of racemate; Enzymatic reaction

3: dicyclohexyl-carbodiimide; dmap / dichloromethane

With dmap; sodium tetrahydroborate; amano PS (native lipase from B_. cepacia earlier Pseudomonas cepacia); dicyclohexyl-carbodiimide; In methanol; dichloromethane; toluene;
DOI:10.1016/j.tet.2013.04.014

Reference yield:

: 75235-71-1,244221-77-0
(+/-)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-ol

: 1433187-97-3
(2R)-1-(1,3-benzothiazol-2-ylsulfanyl)propan-2-yl (2R)-methoxy(phenyl)ethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: amano PS (native lipase from B_. cepacia earlier Pseudomonas cepacia) / toluene / 306 h / 32 °C / Resolution of racemate; Enzymatic reaction

2: dicyclohexyl-carbodiimide; dmap / dichloromethane

With dmap; amano PS (native lipase from B_. cepacia earlier Pseudomonas cepacia); dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1016/j.tet.2013.04.014