2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate

Base Information

Chemical Name:2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate
CAS No.:172977-71-8
Molecular Formula:C₁₆H₂₂N₂O₃Si
Molecular Weight:318.448
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Chemical Property of 2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate

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Technology Process of 2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate

There total 2 articles about 2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 527-60-6
Mesitol

: 172977-71-8
2,4,6-Trimethylphenyl 3-(trimethylsiloxy)-2-diazo-3-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / sodium acetate, tosyl azide / acetone; acetonitrile / 12 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

With 4-toluenesulfonyl azide; sodium acetate; triethylamine; In dichloromethane; acetone; acetonitrile;
DOI:10.1021/jo00128a027