C₂₇H₃₁NO₄

Base Information

Chemical Name:C₂₇H₃₁NO₄
CAS No.:1361131-73-8
Molecular Formula:C₂₇H₃₁NO₄
Molecular Weight:433.547
Hs Code.:

C<sub>27</sub>H<sub>31</sub>NO<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₇H₃₁NO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₁NO₄

Chemical Property:

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Technology Process of C₂₇H₃₁NO₄

There total 1 articles about C₂₇H₃₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1361131-73-8
C₂₇H₃₁NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: chloro-trimethyl-silane / Inert atmosphere

2: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran; dimethyl sulfoxide / 12 h / Inert atmosphere; Reflux

With chloro-trimethyl-silane; sodium hydrogencarbonate; sodium iodide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497

Reference yield:

: 1361131-73-8
C₂₇H₃₁NO₄

: 1361131-78-3
C₂₅H₂₉NO₃

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 6h; Inert atmosphere;
DOI:10.1002/adsc.201100497

Reference yield:

: 1361131-73-8
C₂₇H₃₁NO₄

: C₂₅H₂₇NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

2.1: oxalyl dichloride / dichloromethane; dimethyl sulfoxide / -63 °C / Inert atmosphere

2.2: 0.5 h / Inert atmosphere

3.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C / Inert atmosphere

4.1: boron trifluoride phosphoric acid / dichloromethane / 6 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; oxalyl dichloride; boron trifluoride phosphoric acid; methyllithium; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497