1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

Base Information

Chemical Name:1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate
CAS No.:1639123-26-4
Molecular Formula:C₂HF₃O₂*C₃₃H₃₉N₅
Molecular Weight:619.73
Hs Code.:

1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

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Chemical Property of 1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

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Technology Process of 1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

There total 4 articles about 1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613405-04-1
(E)-3-(1H-benzo[d]imidazol-2-yl)-1-phenylprop-2-en-1-one

: 1639123-26-4
1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 70 °C

2.1: acetic acid / toluene / 3 h / 100 °C / Microwave irradiation

3.1: caesium carbonate / acetonitrile / 50 °C

3.2: C₁₈-RP column

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; caesium carbonate; acetic acid; triethylamine; In ethanol; toluene; acetonitrile; 1.1: |Stetter 1,4-Dicarbonyl Synthesis / 2.1: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1021/jm500632s

Reference yield:

: 3314-30-5
1H-benzoimidazole-2-carboxaldehyde

: 1639123-26-4
1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N-dimethyl-formamide / 60 °C

2.1: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 70 °C

3.1: acetic acid / toluene / 3 h / 100 °C / Microwave irradiation

4.1: caesium carbonate / acetonitrile / 50 °C

4.2: C₁₈-RP column

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; caesium carbonate; acetic acid; triethylamine; In ethanol; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: |Wittig Olefination / 2.1: |Stetter 1,4-Dicarbonyl Synthesis / 3.1: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1021/jm500632s

Reference yield:

: 1613405-05-2
3-(1H-benzo[d]imidazol-2-yl)-5-methyl-1-phenylhexane-1,4-dione

: 1639123-26-4
1-(cyclopentylmethyl)-2-(2-isopropyl-1-(3-(2-methyl-1H-imidazol-1-yl)propyl)-5-phenyl-1H-pyrrol-3-yl)-1H-benzo[d]imidazole trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / toluene / 3 h / 100 °C / Microwave irradiation

2.1: caesium carbonate / acetonitrile / 50 °C

2.2: C₁₈-RP column

With caesium carbonate; acetic acid; In toluene; acetonitrile; 1.1: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1021/jm500632s