(E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride

Base Information

• Chemical Name: (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride
• CAS No.: 305382-64-3
• Molecular Formula: C₂₄H₂₂O₃S
• Molecular Weight: 390.503
• Mol file: 305382-64-3.mol

Synonyms:

Chemical Property of (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride

There total 2 articles about (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Dicyclopropylmethylene-4-[1-(2-methyl-5-phenyl-furan-3-yl)-eth-(Z)-ylidene]-dihydro-furan-2,5-dione → (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride (305382-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaHS / toluene / 4 h / Heating

2: toluene / UV-irradiation

With sodium hydrogensulfide; In toluene; 1: Substitution / 2: Isomerization;

DOI:10.1039/b002033h

Reference yield:

(Z)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride → (E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride (305382-64-3)

Guidance literature:

In toluene; UV-irradiation;

DOI:10.1039/b002033h

Reference yield:

(E)-4-Dicyclopropylmethylene[1-(2-methyl-5-phenyl-3-furyl)ethylidene]thiosuccinic anhydride (305382-64-3) → 8,8-dicyclopropyl-4,8a-dimethyl-2-phenyl-8,8a-dihydro-1-oxa-6-thia-s-indacene-5,7-dione

Guidance literature:

In toluene; UV-irradiation;

DOI:10.1039/b002033h