ClPh₂GeSiPh₃

Base Information

Chemical Name:ClPh₂GeSiPh₃
CAS No.:149033-91-0
Molecular Formula:C₃₀H₂₅ClGeSi
Molecular Weight:521.657
Hs Code.:

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Chemical Property of ClPh₂GeSiPh₃

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Technology Process of ClPh₂GeSiPh₃

There total 1 articles about ClPh₂GeSiPh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.5%

: 15487-82-8,6735-25-7
triphenylsilylkalium

: 1613-66-7
dichlorodiphenylgermane

: 149033-91-0
ClPh₂GeSiPh₃

Guidance literature:: With HCl; In diethyl ether; room temperature; equimolar amounts; addition of KSiPh3 in ether to the germane in ether within 10 min; stirring was continued for 5 min; neutralization with 1 N HCl;; crystn of the product from the ether layer at -18 ° C; elem. anal.;;
DOI:10.1016/0022-328X(93)80184-D

Reference yield: 18.0%

: 149033-91-0
ClPh₂GeSiPh₃

: 57482-41-4
Triphenylgermyl-kalium

: 149033-89-6
Ph₃SiGePh₂GePh₃

Guidance literature:: With Na₂SO₄; HCl; In diethyl ether; addn. of KGe(C6H5)3 in ether to a solution of the silyl germane at -78 ° C within 30 min; stirring for 2 h; the mixture was allowed to warm to room temperature; addn. of 1 N HCl;; filtration; the ether layer was dried over Na2SO4; solvent removal; recrystn. from toluene/heptane; elem. anal.;;
DOI:10.1016/0022-328X(93)80184-D