Technology Process of C39H60N3OSSi2Y
There total 6 articles about C39H60N3OSSi2Y which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium cyanoborohydride; acetic acid / methanol; tetrahydrofuran
2: bis(dibenzylideneacetone)-palladium(0); triphenylphosphine / toluene / 20 h / Reflux
3: toluene / 2 h / 0 °C
4: tetrahydrofuran; hexane / 6 h / 50 °C
With
sodium cyanoborohydride; acetic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; methanol; hexane; toluene;
2: |Stille Cross Coupling;
DOI:10.1002/chem.201303853
- Guidance literature:
-
Multi-step reaction with 5 steps
1: formic acid / methanol / Reflux
2: sodium cyanoborohydride; acetic acid / methanol; tetrahydrofuran
3: bis(dibenzylideneacetone)-palladium(0); triphenylphosphine / toluene / 20 h / Reflux
4: toluene / 2 h / 0 °C
5: tetrahydrofuran; hexane / 6 h / 50 °C
With
formic acid; sodium cyanoborohydride; acetic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; methanol; hexane; toluene;
3: |Stille Cross Coupling;
DOI:10.1002/chem.201303853
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis(dibenzylideneacetone)-palladium(0); triphenylphosphine / toluene / 20 h / Reflux
2: toluene / 2 h / 0 °C
3: tetrahydrofuran; hexane / 6 h / 50 °C
With
triphenylphosphine; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; hexane; toluene;
1: |Stille Cross Coupling;
DOI:10.1002/chem.201303853
