C₁₈H₂₁NO₄

Base Information

Chemical Name:C₁₈H₂₁NO₄
CAS No.:1415019-80-5
Molecular Formula:C₁₈H₂₁NO₄
Molecular Weight:315.369
Hs Code.:

C<sub>18</sub>H<sub>21</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₁NO₄

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₈H₂₁NO₄

There total 3 articles about C₁₈H₂₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157371-82-9
(2,4,10-trioxaadamantylmethyl)phenylcarbinol

: 1415019-80-5
C₁₈H₂₁NO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2-iodoxybenzoic acid / ethyl acetate / 4 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

2.2: 4 h / Reflux

3.1: hydroxylamine hydrochloride; pyridine / ethanol / 3 h / Reflux

4.1: triethylamine / dichloromethane / 2 h / -10 °C

5.1: aluminum oxide / chloroform / 2 h / Reflux

With pyridine; aluminum oxide; 2-iodoxybenzoic acid; hydroxylamine hydrochloride; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; chloroform; ethyl acetate; 5.1: |Beckmann Rearrangement;
DOI:10.3762/bjoc.8.161

Reference yield:

: 1415019-65-6
C₁₈H₂₀O₄

: 1415019-80-5
C₁₈H₂₁NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 3 h / Reflux

2: triethylamine / dichloromethane / 2 h / -10 °C

3: aluminum oxide / chloroform / 2 h / Reflux

With pyridine; aluminum oxide; hydroxylamine hydrochloride; triethylamine; In ethanol; dichloromethane; chloroform; 3: |Beckmann Rearrangement;
DOI:10.3762/bjoc.8.161

Reference yield:

: 157371-83-0
3-phenacyl-2,4,10-trioxaadamantane

: 1415019-80-5
C₁₈H₂₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

1.2: 4 h / Reflux

2.1: hydroxylamine hydrochloride; pyridine / ethanol / 3 h / Reflux

3.1: triethylamine / dichloromethane / 2 h / -10 °C

4.1: aluminum oxide / chloroform / 2 h / Reflux

With pyridine; aluminum oxide; hydroxylamine hydrochloride; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; chloroform; 4.1: |Beckmann Rearrangement;
DOI:10.3762/bjoc.8.161