C₆₃H₆₅N₅O₈

Base Information

• Chemical Name: C₆₃H₆₅N₅O₈
• CAS No.: 1354328-31-6
• Molecular Formula: C₆₃H₆₅N₅O₈
• Molecular Weight: 1020.24
• Mol file: 1354328-31-6.mol

Synonyms:

Chemical Property of C₆₃H₆₅N₅O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₃H₆₅N₅O₈

There total 12 articles about C₆₃H₆₅N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide (53008-62-1,53008-61-0) + C29H31N5O3 → C63H65N5O8 (1354328-31-6)

Guidance literature:

C₂₉H₃₁N₅O₃; With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In benzene; at 65 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;

2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide; In benzene; at 65 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ml200278u

Reference yield:

C16H18N2O2 → C63H65N5O8 (1354328-31-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

2.1: methanol / 3 h / 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 4 h / 120 °C / Inert atmosphere; Microwave irradiation

5.1: toluene-4-sulfonic acid / methanol / 5 h / 20 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / benzene / 0.17 h / 65 °C / Inert atmosphere; Molecular sieve

6.2: 3 h / 65 °C / Inert atmosphere

With sodium azide; palladium on activated charcoal; hydrogen; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; benzene;

DOI:10.1021/ml200278u

Reference yield:

C49H48N2O6S → C63H65N5O8 (1354328-31-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium azide / N,N-dimethyl-formamide / 4 h / 120 °C / Inert atmosphere; Microwave irradiation

2.1: toluene-4-sulfonic acid / methanol / 5 h / 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / benzene / 0.17 h / 65 °C / Inert atmosphere; Molecular sieve

3.2: 3 h / 65 °C / Inert atmosphere

With sodium azide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; benzene;

DOI:10.1021/ml200278u

upstream raw materials:

C₄₈H₄₆N₂O₄

2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide

C₄₀H₃₆O₅

4-methyl-benzaldehyde