C₂₀H₂₂⁽²⁾HNO

Base Information

Chemical Name:C₂₀H₂₂⁽²⁾HNO
CAS No.:1416465-89-8
Molecular Formula:C₂₀H₂₃NO
Molecular Weight:294.401
Hs Code.:

C<sub>20</sub>H<sub>22</sub><sup>(2)</sup>HNO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₂⁽²⁾HNO

Chemical Property:

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Technology Process of C₂₀H₂₂⁽²⁾HNO

There total 4 articles about C₂₀H₂₂⁽²⁾HNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1416465-75-2
N-benzyl-N-(2-bromoallyl)-2-methyl-3-phenylpropanamide

: 1416465-89-8
C₂₀H₂₂⁽²⁾HNO

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tributyltin deuteride; In toluene; for 2.5h; Reflux; Inert atmosphere;
DOI:10.1139/v2012-085

Reference yield:

: 1199-77-5
α-methylcinnamic acid

: 1416465-89-8
C₂₀H₂₂⁽²⁾HNO

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C / Inert atmosphere

2: oxalyl dichloride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

3: triethylamine / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

4: 2,2'-azobis(isobutyronitrile); tributyltin deuteride / toluene / 2.5 h / Reflux; Inert atmosphere

With oxalyl dichloride; 2,2'-azobis(isobutyronitrile); palladium 10% on activated carbon; hydrogen; tributyltin deuteride; triethylamine; In diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1139/v2012-085

Reference yield:

: 1009-67-2
2-methyl-3-phenylpropanoic acid

: 1416465-89-8
C₂₀H₂₂⁽²⁾HNO

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere

3: 2,2'-azobis(isobutyronitrile); tributyltin deuteride / toluene / 2.5 h / Reflux; Inert atmosphere

With oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tributyltin deuteride; triethylamine; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1139/v2012-085