{(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester
• CAS No.: 53317-24-1
• Molecular Formula: C₃₀H₄₀Cl₄N₆O₆S₂
• Molecular Weight: 786.628

Synonyms:

Chemical Property of {(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester

Chemical Property:

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Technology Process of {(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester

There total 4 articles about {(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzyl chloroformate (501-53-1,94274-21-2) + cydrine (53317-25-2,57357-12-7) → {(R)-2-{(R)-2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester (53317-24-1)

Guidance literature:

In pyridine; 15 min, -10 deg C; 30 min, 0-4 deg C;

Reference yield: 68.2%

1,1-bis-(2-chloroethyl)-hydrazine (10487-06-6) + (S)-2-Benzyloxycarbonylamino-3-{2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-propionic acid → {(S)-2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester (53317-24-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; 1) 4 h, 0 degC; 2) 1 h, room temp.;

Reference yield: 62.0%

1,1-bis-(2-chloroethyl)-hydrazine (10487-06-6) + 2-Benzyloxycarbonylamino-3-{2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-propionic acid → {2-{2-Benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-1-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl}-carbamic acid benzyl ester (53317-24-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; 1) 4 h, 0 degC; 2) 1 h, room temp.;

upstream raw materials:

1,1-bis-(2-chloroethyl)-hydrazine

benzyl chloroformate

cydrine

Downstream raw materials:

2-Amino-3-{2-amino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

(S)-2-Amino-3-{2-amino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyldisulfanyl}-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

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