tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name)

Base Information

Chemical Name:tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name)
CAS No.:32899-48-2
Molecular Formula:C₁₇H₂₆N₄O₅
Molecular Weight:366.417
Hs Code.:

Synonyms:Serine,N-(N-carboxy-3-phenyl-L-alanyl)-, N-tert-butyl ester, hydrazide, L- (8CI); NSC343956

Suppliers and Price of tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name)

Chemical Property:

Vapor Pressure:2.17E-20mmHg at 25°C
Boiling Point:696.9°C at 760 mmHg
Flash Point:375.3°C
Density:1.233g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name)

There total 3 articles about tert-butyl {1-[(1-hydrazinyl-3-hydroxy-1-oxopropan-2-yl)amino]-1-oxo-3-phenylpropan-2-yl}carbamate (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 34290-59-0
(S)-methyl 2-((2S)-2-[(tert-butoxycarbonyl)-3-phenylpropanamido]-3-hydroxy)-propanoate

: 32899-48-2
Boc-Phe-Ser-NHNH₂

Guidance literature:: With hydrazine hydrate; Ambient temperature;
DOI:10.1246/bcsj.64.1533

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 32899-48-2
Boc-Phe-Ser-NHNH₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NMM, ethyl chloroformate, 2) NMM / 1) THF, 2) DMF, r.t.

2: 54 percent / 80percent hydrazine hydrate / Ambient temperature

With 4-methyl-morpholine; chloroformic acid ethyl ester; hydrazine hydrate;
DOI:10.1246/bcsj.64.1533