phenyl(1-phenylethynyl)mesitylstibine

Base Information

Chemical Name:phenyl(1-phenylethynyl)mesitylstibine
CAS No.:757959-99-2
Molecular Formula:C₂₃H₂₁Sb
Molecular Weight:419.17
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl(1-phenylethynyl)mesitylstibine

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Technology Process of phenyl(1-phenylethynyl)mesitylstibine

There total 1 articles about phenyl(1-phenylethynyl)mesitylstibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 114812-75-8
phenyldiethynylstibine

: 2633-66-1
2-mesitylmagnesium bromide

: 757959-99-2
phenyl(1-phenylethynyl)mesitylstibine

Guidance literature:: In diethyl ether; 2,4,6-trimethylphenyl magnesiumbromide at 0°C added under N2 to stirred soln. of phenyldiethynylstibine in dry ether; react. mixt. stirred for 6 h and then diluted with hexane and water; org. layer washed withsoln. of NaCl and dried over Na2SO4; solvent removed in vac. and residue eluted in silica gel column chromy. (hexane);
DOI:10.1016/j.molcata.2007.04.018