(eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

Base Information

Chemical Name:(eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]
CAS No.:885334-12-3
Molecular Formula:C₂₄H₄₃Cl₂N₂NbSi₃
Molecular Weight:607.688
Hs Code.:

(eta.5-C<sub>5</sub>H<sub>4</sub>SiMe<sub>3</sub>)NbCl<sub>2</sub>[NC<sub>6</sub>Me<sub>4</sub>-4-(N(SiMe<sub>3</sub>)2)]

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Chemical Property of (eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

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Technology Process of (eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

There total 1 articles about (eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 885334-07-6
N,N,N',N'-tetrakis(trimethylsilyl)-2,3,5,6-tetramethyl-1,4-phenylenediamine

: (η5-trimethylsilylcyclopentadienyl)niobium tetrachloride

: 885334-12-3
(eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

Guidance literature:: In dichloromethane; (N2); heating mixture of niobium compd. and amine in molar ratio 1:1 in CH2Cl2 at 90°C for 48 h, evapn., addn. of CH2Cl2, heating at 90°C for 16 h, repeating of process (evapn., addn. CH2Cl2, heating at90°C for 16 h) 2 more times; evapn., extn. (hexane), recrystn. (hexane), elem. anal.;
DOI:10.1016/j.jorganchem.2005.12.016

Reference yield: 96.0%

: 885334-12-3
(eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

: lithium trimethylsilylcyclopentadienide

: 885334-13-4
(η5-C5H4SiMe3)2NbCl(NC6Me4-4-(N(SiMe3)2))

Guidance literature:: In hexane; (N2); addn. of suspn. of lithium compd. in hexane to soln. of niobium compd. in hexane at -78°C, stirring at room temp. for 12 h; filtration, evapn., elem. anal.;
DOI:10.1016/j.jorganchem.2005.12.016

Reference yield: 89.0%

: 885334-12-3
(eta.5-C₅H₄SiMe₃)NbCl₂[NC₆Me₄-4-(N(SiMe₃)2)]

: 3585-33-9
lithium dimethylamide

: 885334-15-6
(η5-C5H4SiMe3)NbCl(NMe2)[NC6Me4-4-(N(SiMe3)2)]

Guidance literature:: In diethyl ether; (N2); addn. of suspn. of lithium compd. in ether to soln. of niobium compd. in hexane at -78°C, stirring at room temp. for 12 h; filtration, evapn., elem. anal.;
DOI:10.1016/j.jorganchem.2005.12.016