Technology Process of C15H18O3
There total 4 articles about C15H18O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ozone; acetic acid / ethyl acetate; water / 0 °C / Inert atmosphere
2.1: sulfuric acid / Dean-Stark; Reflux; Inert atmosphere
3.1: allyl alcohol; potassium / toluene / Reflux; Inert atmosphere
3.2: Reflux; Inert atmosphere
With
sulfuric acid; potassium; ozone; acetic acid; allyl alcohol;
In
water; ethyl acetate; toluene;
3.1: |Dieckmann Condensation;
DOI:10.1002/asia.201301248
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sulfuric acid / Dean-Stark; Reflux; Inert atmosphere
2.1: allyl alcohol; potassium / toluene / Reflux; Inert atmosphere
2.2: Reflux; Inert atmosphere
With
sulfuric acid; potassium; allyl alcohol;
In
toluene;
2.1: |Dieckmann Condensation;
DOI:10.1002/asia.201301248
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium iodide / acetone / 7 h / Reflux; Inert atmosphere
2.1: allyl alcohol; potassium / toluene / Reflux; Inert atmosphere
2.2: Reflux; Inert atmosphere
With
potassium; allyl alcohol; sodium iodide;
In
acetone; toluene;
2.1: |Dieckmann Condensation;
DOI:10.1002/asia.201301248