bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)

Base Information

Chemical Name:bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)
CAS No.:1122709-05-0
Molecular Formula:C₄₀H₃₀Cl₄N₂O₂Sn
Molecular Weight:831.212
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)

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Technology Process of bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)

There total 1 articles about bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 3002-01-5
dibenzyltin(IV) dichloride

: 161696-84-0
N-(3,5-dichlorosalicylidene)aniline

: 1122709-05-0
bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)

Guidance literature:: With NaH; In tetrahydrofuran; under N2, Schlenk or glove-box techniques; soln. of org. ligand (4.13 mmol) added to NaH soln. (2.06 mmol) (0°C); warmed to room temp.; stirred; added to soln. of Cl2Sn(CH2Ph)2 (2.06 mmol) (0°C); warmedto room temp.; stirred overnight; solvent removed (vac.); extd. with toluene; concd.; stored (-20°C) overnight; elem. anal.;
DOI:10.1002/ejic.200700937

Reference yield:

: 1122709-05-0
bis[N-(3,5-dichlorosalicylidene)anilinato]dibenzyltin(IV)

: 1109-15-5
tris(pentafluorophenyl)borate

: 1122709-09-4
(bis[N-(3,5-dichlorosalicylidene)anilinato]benzyltin(IV))⁽¹⁺⁾

Guidance literature:: In dichloromethane-d2; under N2 using Schlenk or glove-box techniques; Sn complex (18 μmol) dissolved in dry CD2Cl2; B(C6F5)3 (18 μmol) added; not isolated; analyzed by NMR;
DOI:10.1002/ejic.200700937